This paper deals with the fire assay concentration and ICP spectrographic methods for analyzing trace platinummetals and gold in copper and nickel sulphide minerals. Samples were treated by sulphur and stibium assay concentration.The stibiuni buttons were subjected to cupellation until a diameter of some 1 .5 mm was obtained.Some stibium powder was added to the buttons, and ground to 200-300 mesh.They were analyzed directly with an ICP automatic spectromet- er.