Extraction-Spectrophotometric Determination of Niobium at Microgram level in ores with 5一Br一PADAP
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A method of determination of niobium in the form of Nb-Br-PADAP-tart- rate complex extracted with n-butyl alcohol is described. The interference of tantalum is eliminated by increasing the amounts of tartaric acid, and the color is stable for at least 40 hours. The detection limit is 0.01 µg/ml, and the C. V.% is 4 .9% for 10 determinations with sample containing 0.054% of Nb2O5.
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吴曼君, 1982. 5-Br-PADAP萃取分光光度法测定矿石中微克量铌[J]. 岩石矿物学杂志, 1(3):56~60. , 1982. Extraction-Spectrophotometric Determination of Niobium at Microgram level in ores with 5一Br一PADAP[J]. Acta Petrologica et Mineralogica, 1(3): 56~60.